Title
(S)-2-Oxotetra-hydro-furan-3-aminium bromide
Document Type
Article
Publication Date
8-1-2012
Abstract
In the title HBr salt of (S)-homoserine lactone, C(4)H(8)NO(2) (+)·Br(-), the five-membered ring has an envelope conformation, with the -CH(2)- C atom adjacent to the N-substituted C atom at the flap position. The four-atom mean plane (r.m.s. deviation = 0.005 Å) of the envelope forms a dihedral angle of 32.12 (9)° with the three-atom flap plane. The distorted square-pyramidal coordination about the anion involves five surrounding cations, with the square base defined by three N-H⋯Br hydrogen bonds [Br⋯N = 3.3046 (10), 3.3407 (12) and 3.3644 (13) Å] and near-contact with an H atom attached to C [Br⋯C = 3.739 (1) Å]. Another Br⋯C contact of 3.427 (1) Å defines the apex. There is also an N-H⋯O hydrogen bond present linking the cations.
Publication Source (Journal or Book title)
Acta crystallographica. Section E, Structure reports online
First Page
o2539
Recommended Citation
Sandifer, J. D., Fronczek, F. R., & Watkins, S. F. (2012). (S)-2-Oxotetra-hydro-furan-3-aminium bromide. Acta crystallographica. Section E, Structure reports online, 68 (Pt 8), o2539. https://doi.org/10.1107/S1600536812032552