Synthesis of a silicone-containing flame retardant and its application in flame retarding polycarbonate

Document Type

Article

Publication Date

10-1-2011

Abstract

Hydrogen-containing silicone oil modified with phenol (HSOP) was used to improve the flame retardancy of polycarbonate (PC). Flame-retardant and mechanical properties results show that when the HSOP content is 5%, the limiting oxygen index (LOI) values of PC increase from 26.5% to 32.5% and vertical burning rating (UL-94) enhances from V-2 rating to V-0 rating, notched impact strength and breaking elongation increases 48.9% and 37.6% respectively. The possible flame retardant mechanism of HSOP was studied via thermogravimetric analysis (TGA) measurements on PC/HSOP and scanning electron microscopy (SEM) observation on char residues. The results demonstrate that dense char layer formed by cross-linking between the HSOP and PC matrix during combustion is crucial to improve the flame retardancy of materials.

Publication Source (Journal or Book title)

Gaofenzi Cailiao Kexue Yu Gongcheng/Polymeric Materials Science and Engineering

First Page

138

Last Page

142

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